Hi sangam56,
This shouldn't be too difficult to accomplish. Have you built your TreeView already? If not check out
this which I found very useful the first time that I used the control.
Once you've built your TreeView you need to use the OnSelectedNodeChanged event to fire a sub which will work out which node you've clicked and populate your GridView accordingly. Use the TreeView1.SelectedNode.Value property to find out which node was clicked.
Let me know how you get on,
Dr B
P.S. You posted this in the ASP Forum which is for Classic ASP only. I've moved it for you but in future please post all your ASP.NET questions in the .NET Forum. Thanks.